WANG Yanni,LV Huangzhen,LI Pingting,et al.Uncertainty evaluation of determination of methomyl residues in potato by high performance liquid chromatography-tandem mass spectrometry[J].Agricultural Engineering,2023,13(12):72-76. DOI: 10.19998/j.cnki.2095-1795.2023.12.013
Citation: WANG Yanni,LV Huangzhen,LI Pingting,et al.Uncertainty evaluation of determination of methomyl residues in potato by high performance liquid chromatography-tandem mass spectrometry[J].Agricultural Engineering,2023,13(12):72-76. DOI: 10.19998/j.cnki.2095-1795.2023.12.013

Uncertainty Evaluation of Determination of Methomyl Residues in Potato by High Performance Liquid Chromatography-Tandem Mass Spectrometry

  • In order to improve accuracy of potato food safety detection results, high performance liquid chromatography-tandem mass spectrometry was used to determine methomyl in potato, analyze specific experimental process, establish a mathematical model, determine and compare components of measurement uncertainty.When residue of aphid phosphorus in potato was 1.3 μg/kg, expanded uncertainty was 0.84 μg/kg(k=2).Results showed that among measurement uncertainty components, uncertainty caused by instrument itself, standard curve drawing and experimental repeatability were main factors.
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