Uncertainty Evaluation of Determination of Methomyl Residues in Potato by High Performance Liquid Chromatography-Tandem Mass Spectrometry
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Graphical Abstract
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Abstract
In order to improve accuracy of potato food safety detection results, high performance liquid chromatography-tandem mass spectrometry was used to determine methomyl in potato, analyze specific experimental process, establish a mathematical model, determine and compare components of measurement uncertainty.When residue of aphid phosphorus in potato was 1.3 μg/kg, expanded uncertainty was 0.84 μg/kg(k=2).Results showed that among measurement uncertainty components, uncertainty caused by instrument itself, standard curve drawing and experimental repeatability were main factors.
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